Cyanuric chloride → 2,4-Dichloro-6-methoxy-3,5-triazine

HRID 622469

Reaction equation

HRID 622469 reaction equation
[C:1](=O)([O-])[OH:2].[Na+].[N:6]1[C:13]([Cl:14])=[N:12][C:10]([Cl:11])=[N:9][C:7]=1Cl>CO>[CH3:1][O:2][C:7]1[N:9]=[C:10]([Cl:11])[N:12]=[C:13]([Cl:14])[N:6]=1

Participants

4

Reactant 2

HCID 7954Cyanuric chlorideHCID 516892Sodium Bicarbonate

Product 1

HCID 192672,4-Dichloro-6-methoxy-3,5-triazine

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
0 °C

Procedure

7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.

Workup

  1. customa reaction for 60 minutes
  2. custom(First condensation)
  3. customthe crystal precipitated
  4. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-746073f0754f43e5a068c64e1aa9eb68
Source dataset
uspto-grants-1988_09
Patent number
US04771132

Linked notes

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