Cyanuric chloride → 2,4-Dichloro-6-methoxy-3,5-triazine
Reaction equation
[C:1](=O)([O-])[OH:2].[Na+].[N:6]1[C:13]([Cl:14])=[N:12][C:10]([Cl:11])=[N:9][C:7]=1Cl>CO>[CH3:1][O:2][C:7]1[N:9]=[C:10]([Cl:11])[N:12]=[C:13]([Cl:14])[N:6]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 0 °C
Procedure
7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.
Workup
- customa reaction for 60 minutes
- custom(First condensation)
- customthe crystal precipitated
- filtrationwas collected by filtration
Sources & evidence
- ORD record
- ord-746073f0754f43e5a068c64e1aa9eb68
- Source dataset
- uspto-grants-1988_09
- Patent number
- US04771132
Reaction notes
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