1,6-Hexanediol → 1,6-Hexanediol adipoyl chloride

HRID 636792

Reaction equation

HRID 636792 reaction equation
[C:1]([Cl:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([Cl:8])=[O:7].C(O)CCCCCO>C(N(CC)CC)C>[CH2:1]([OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][OH:7].[C:1]([Cl:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([Cl:8])=[O:7]

Participants

4

Reactant 2

HCID 123741,6-HexanediolHCID 61034Adipoyl chloride3×

Product 1

HCID 867564751,6-Hexanediol adipoyl chloride

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Next, the adipoyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 3 minutes. Consequently, adipoyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between adipoyl chloride condensed on the surface of the base particles and 1,6-hexanediol contained therein, forming a film of 1,6-hexanediol-adipoyl chloride co-polymer on the surface of the base particles.

Workup

  1. customA polymerization reaction

Sources & evidence

ORD record
ord-7d3f9ba074624e8a96aaeab24379b4c5
Source dataset
uspto-grants-2001_02
Patent number
US06194487B1

Linked notes

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