Dimethyl Sulfoxide → 2-Acetyl-6-methylpyridine

HRID 813144

Reaction equation

HRID 813144 reaction equation
[CH2:28]([Cl:29])[Cl:30].[CH3:11][c:12]1[cH:13][cH:14][cH:15][c:16]([CH:18]([CH3:19])[OH:20])[n:17]1.[CH3:21][CH2:22][N:23]([CH2:24][CH3:25])[CH2:26][CH3:27].[CH3:7][S:8]([CH3:9])=[O:10].[Cl:1][C:2]([C:3]([Cl:4])=[O:5])=[O:6]>>[CH3:11][c:12]1[cH:13][cH:14][cH:15][c:16]([C:18]([CH3:19])=[O:20])[n:17]1

Participants

6

Reactant 5

HCID 679Dimethyl SulfoxideHCID 6344DichloromethaneHCID 8471TriethylamineHCID 65578Oxalyl chlorideHCID 3531381-(6-Methylpyridin-2-yl)ethanol

Product 1

HCID 1388722-Acetyl-6-methylpyridine

Sources & evidence

ORD record
ord-93a8aecd2d5d464aa0e775a78c6b7514
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Linked notes

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