Benzyl chloroformate → Benzyl hydroxycarbamate

HRID 971451

Reaction equation

Cl[C:2]([O:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=[O:3].Cl.[NH2:13][OH:14]>>[CH2:5]([O:4][C:2](=[O:3])[NH:13][OH:14])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

Reactant 2

HCID 10387Benzyl chloroformate

HCID 443297Hydroxyamine hydrochloride

Product 1

HCID 18907Benzyl hydroxycarbamate

Procedure

170.5 parts of benzyl chloroformate are reacted with 69.5 parts of ground hydroxylamine hydrochloride in a similar manner to Example 8 to give 149 parts of benzyl-N-hydroxycarbamate as a waxy solid.

Sources & evidence

ORD record: ord-b6ba9e94aa4e40d792a3e351be571685
Source dataset: uspto-grants-1979_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04160077

Linked notes

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