Diethylhydroxylamine → HCID 54273460, compound

HRID 979262

Reaction equation

HRID 979262 reaction equation
[CH2:1]([N:3]([CH2:5][CH3:6])[OH:4])[CH3:2].[CH2:7]([O:25][C:26](=[O:29])[CH:27]=[CH2:28])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].CC(C)([O-])C.[K+]>O1CCCC1>[CH2:7]([O:25][C:26](=[O:29])[CH2:27][CH2:28][O:4][N:3]([CH2:5][CH3:6])[CH2:1][CH3:2])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

5

Reactant 3

HCID 19463DiethylhydroxylamineHCID 62552Stearyl acrylateHCID 23665647Potassium tert-butoxide

Product 1

HCID 54273460HCID 54273460, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The procedure of Example I is repeated using 4.46 g of N,N-diethylhydroxylamine, 16.03 g of n-octadecylacrylate and 0.56 g of potassium-tert-butoxide in 100 ml of tetrahydrofuran, to afford the title compound as a colorless liquid.

Sources & evidence

ORD record
ord-fc5a3342fe564b3fa23ee63fe449222b
Source dataset
uspto-grants-1987_05
Patent number
US04666962

Linked notes

Loading…