2,4-Dinitroaniline → 6-Chloro-N-(2,4-dinitrophenyl)-3-pyridinecarboxamide

HRID 1007193

反応式

HRID 1007193 の反応式
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[N+:11]([C:14]1[CH:20]=[C:19]([N+:21]([O-:23])=[O:22])[CH:18]=[CH:17][C:15]=1[NH2:16])([O-:13])=[O:12]>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:16][C:15]2[CH:17]=[CH:18][C:19]([N+:21]([O-:23])=[O:22])=[CH:20][C:14]=2[N+:11]([O-:13])=[O:12])=[O:7])=[CH:9][CH:10]=1

参加物

3

反応物 2

HCID 73212,4-DinitroanilineHCID 27821656-Chloronicotinoyl Chloride

生成物 1

HCID 226689356-Chloro-N-(2,4-dinitrophenyl)-3-pyridinecarboxamide

実験手順

The title compound was prepared from 6-chloronicotinoyl chloride and 2,4-dinitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.69 (bs, 1H), 9.28-9.23 (m, 2H), 9.06-9.05 (m, 1H), 8.61-8.57 (m, 1H), 8.28-8.24 (m, 1H), 7.59-7.56 (m, 1H).

後処理

  1. customwas obtained as a yellow solid

出典と根拠

ORDレコード
ord-9467038bc9184c648988a41feae5a4d7
出典データセット
uspto-grants-2004_09
特許番号
US06794397B2

関連ノート

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