Methyl iodide → HCID 178503575、化合物
反応式
[Cl:1][C:2]1[C:3](=[S:9])[NH:4][C:5](=[O:8])[NH:6][CH:7]=1.[CH3:10]I>[H-].[Na+]>[CH3:10][S:9][C:3]1[C:2]([Cl:1])=[CH:7][NH:6][C:5](=[O:8])[N:4]=1参加物
4
実験手順
5-Chloro-4-thiouracil (0.0027 mol) was dissolved in 1 M sodium hydride (3 ml) and methyl iodide (0.007 mol) added. The solution was stirred at room temperature for 3 hr. and the solid precipitate collected and recrystallised from water; yield 21%, m.p. 254° C.
後処理
- customand the solid precipitate collected
- customrecrystallised from water
出典と根拠
- ORDレコード
- ord-f0e0bd5863d141bab154410e25b9eb9e
- 出典データセット
- uspto-grants-1983_07
- 特許番号
- US04395406
反応ノート
読み込み中…