反応式
[C:1]([O:7][CH2:8][CH3:9])(=[O:6])[CH2:2][C:3]([CH3:5])=O.[NH:10]1[CH2:14][CH2:13][CH2:12][CH2:11]1>>[NH:10]1[CH2:14][CH2:13][CH2:12][CH:11]1[C:3]([CH3:5])=[CH:2][C:1]([O:7][CH2:8][CH3:9])=[O:6]参加物
3
実験手順
Ethyl 3-tetrahydropyrrolyl-2-butenoate was prepared (21 g, 99%) from ethyl acetoacetate (15.0 g, 115.26 mmol) and pyrrolidine (71.1 mL, 345.78 mmol) in the same manner as described in the above Example 1 (1), and the obtained product was identified with the following NMR data.
出典と根拠
- ORDレコード
- ord-c4f6c0a039404fa9b84557e51bc4c6bf
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07094908B2
関連ノート
読み込み中…