Pyrrolidine → Allyl 3-tetrahydropyrrolyl-2-butenoate

HRID 10836

反応式

HRID 10836 の反応式
[C:1]([O:7][CH2:8][CH:9]=[CH2:10])(=[O:6])[CH2:2][C:3]([CH3:5])=O.[NH:11]1[CH2:15][CH2:14][CH2:13][CH2:12]1>>[NH:11]1[CH2:15][CH2:14][CH2:13][CH:12]1[C:3]([CH3:5])=[CH:2][C:1]([O:7][CH2:8][CH:9]=[CH2:10])=[O:6]

参加物

3

実験手順

Allyl 3-tetrahydropyrrolyl-2-butenoate was prepared (4.7 g, 68%) in the same manner as described in the above Example 1 (1) from allyl acetoacetate (5.0 g, 35.17 mmol) and pyrrolidine (8.8 mL, 105.51 mmol), and the obtained product was identified with the following 1H NMR data.

出典と根拠

ORDレコード
ord-b23c8ba54c484e1bafaf208e0e2e4633
出典データセット
uspto-grants-2006_08
特許番号
US07094908B2

関連ノート

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