Diethyl Carbonate → 4-(Methoxymethyl)-1,3-dioxolan-2-one
反応式
[CH3:1][O:2][CH2:3][CH:4]([OH:7])[CH2:5][OH:6].[C:8](=O)(OCC)[O:9]CC.[H-].[Na+]>>[CH3:1][O:2][CH2:3][CH:4]1[CH2:5][O:6][C:8](=[O:9])[O:7]1参加物
4
実験手順
A mixture of 14 g (0.132 mol) of 3-methoxypropane-1,2-diol (S)and 31.16 g (0.264 mol) of diethyl carbonate in the presence of 0.108 g of 50% sodium hydride is heated until distillation of the alcohol formed. After completion of the reaction, the aimed product is distilled.
後処理
- customformed
- customAfter completion of the reaction
- distillationthe aimed product is distilled
出典と根拠
- ORDレコード
- ord-232a71c783ce456081e5648dee449bfc
- 出典データセット
- uspto-grants-1991_07
- 特許番号
- US05036091
反応ノート
読み込み中…