反応式
[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:3])[CH3:2].[C:10]([C:13]1[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=1)(=[O:12])[CH3:11]>>[OH:12][C:10]([CH3:11])([C:13]1[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=1)[CH2:2][C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])=[O:3]参加物
3
実験手順
A 100 milligram quantity of the hydroxy ester described in Example III is pyrolyzed in a sealed tube at 400° C. for 3 minutes. Analysis of the pyrolysis mixture by gas chromatography indicates the presence of about 30% of a mixture in a 1:1 ratio of amyl acetate and 4-acetylpyridine. The remainder of the mixture contains unreacted starting material.
出典と根拠
- ORDレコード
- ord-f9b23d518ce24be28e1dde3284ee6ee2
- 出典データセット
- uspto-grants-1982_01
- 特許番号
- US04312368
関連ノート
読み込み中…