Azobisisobutyronitrile → Styrene glycidyl Methacrylate

HRID 1166408

反応式

HRID 1166408 の反応式
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:14][CH2:15][CH:16]1[O:18][CH2:17]1)(=[O:13])[C:10]([CH3:12])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>C1(C)C=CC=CC=1>[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9]([O:14][CH2:15][CH:16]1[O:18][CH2:17]1)(=[O:13])[C:10]([CH3:12])=[CH2:11]

参加物

5

反応物 3

HCID 6547AzobisisobutyronitrileHCID 7501StyreneHCID 7837Glycidyl methacrylate

生成物 1

HCID 21867792Styrene glycidyl Methacrylate

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

The same four-necked flask as used in Example 1 was charged with 100 g of toluene, and the temperature was adjusted to 80° C. with stirring under nitrogen. Then, 120 g of styrene, 89 g of glycidyl methacrylate and 0.1 g of azobisisobutyronitrile were added thereto and the reaction carried out in the same manner as in Example 1 to give a styrene-glycidyl methacrylate copolymer. This copolymer (96 weight parts) and 4 weight parts of 4,4′-bisazidobenzal(4-methyl)cyclohexanone were dissolved in 100 weight parts of xylene and the solution was subjected to polymerization in the same manner as in Example 1, whereupon an over coat film was obtained.

後処理

  1. customwas adjusted to 80° C.

出典と根拠

ORDレコード
ord-a6513315a0884485aafab8d4df47f1db
出典データセット
uspto-grants-2003_09
特許番号
US06613855B1

関連ノート

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