Lithium Hydroxide → HCID 23714172、化合物
反応式
[C:1]1([C:7]2[CH:8]=[C:9]([CH:14]=[CH:15][N:16]=2)[C:10]([O:12]C)=[O:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Li+:18]>C1COCC1>[C:1]1([C:7]2[CH:8]=[C:9]([CH:14]=[CH:15][N:16]=2)[C:10]([O-:12])=[O:11])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Li+:18]参加物
4
実験手順
A solution of methyl 2-phenylisonicotinate, N-oxide (397 mg, 1.73 mmol) in THF (6 mL) was treated with 0.5 N aqueous lithium hydroxide (3.65 mL, 1.81 mmol), and the mixture was stirred overnight. The THF was stripped, and the aqueous solution was freeze dried to yield lithium 2-phenylisonicotinate, N-oxide a colorless glass, which was used as-is in the next step.
後処理
- customdried
出典と根拠
- ORDレコード
- ord-72af276ed652451796b3981482abb5af
- 出典データセット
- uspto-grants-2010_11
- 特許番号
- US07829571B2
反応ノート
読み込み中…