反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH:9]=[O:10])=[CH:4][CH:3]=1.S(=O)(=O)(O)[OH:12].Cl[O-].[Na+]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([OH:12])=[O:10])=[CH:4][CH:3]=1参加物
4
実験手順
In the like manner as Example 1, 26.4 g of p-methylphenylacetaldehyde as an aldehyde and 2.3 g of sulfuric acid were used. The oxidation was done by using 125 g of 12% aqueous solution of sodium hypochlorite at temperatures of -10° to -12° C., which was followed by the hydrogenation to obtain p-methylphenylacetic acid.
後処理
- customat temperatures of -10° to -12° C., which
出典と根拠
- ORDレコード
- ord-a6c0e22ac83543e18b5dba56bc8d265d
- 出典データセット
- uspto-grants-1989_03
- 特許番号
- US04814494
関連ノート
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