Triethoxychlorosilane → Acryltriethoxysilane
反応式
[C:1]([O-:5])(=O)[CH:2]=[CH2:3].[Na+].Cl[Si:8]([O:15][CH2:16][CH3:17])([O:12][CH2:13][CH3:14])[O:9][CH2:10][CH3:11]>C1COCC1>[C:1]([Si:8]([O:15][CH2:16][CH3:17])([O:12][CH2:13][CH3:14])[O:9][CH2:10][CH3:11])([CH:2]=[CH2:3])=[O:5]参加物
4
反応条件
- 温度
- -70 °C
実験手順
6.123 g (0.0651 mol) sodium acrylate is dissolved to 25 mL THF and cooled to −70° C. 12.8 mL (0.0651 mol, 12.938 g) chlorotriethoxysilane in THF (15 mL) is added dropwise to reaction solution. The solution is stirred for over night allowing it to warm up to room temperature. NaCl is removed by filtration and solution evaporated to dryness to result clear liquid, acryltriethoxysilane.
後処理
- temperatureto warm up to room temperature
- customNaCl is removed by filtration and solution
- customevaporated to dryness
出典と根拠
- ORDレコード
- ord-ebe86df30b2441388fb356c07f9e4914
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07098346B2
反応ノート
読み込み中…