Nitric Acid → Aluminum nitrate

HRID 1257483

反応式

HRID 1257483 の反応式
[N+:1]([O-:4])([OH:3])=[O:2].O.O.O.O.O.O.O.O.O.[N+:14]([O-:17])([O-:16])=[O:15].[Al+3:18].[N+:19]([O-:22])([O-:21])=[O:20].[N+]([O-])([O-])=O>O>[N+:1]([O-:4])([O-:3])=[O:2].[Al+3:18].[N+:14]([O-:17])([O-:16])=[O:15].[N+:19]([O-:22])([O-:21])=[O:20]

参加物

4

反応物 2

HCID 944Nitric AcidHCID 24567Aluminum nitrate nonahydrate

生成物 1

HCID 26053Aluminum nitrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

An aqueous solution in which 4.16 kg of aluminum nitrate nonahydrate and 540 g of 60% nitric acid were dissolved in 5.0 L of pure water was gradually dropped into 20.0 kg of a stirred silica sol solution having a colloidal particle diameter of from 10 to 20 nm held at 15° C. (Snowtex N-30 manufactured by Nissan Chemical Industries, Ltd. (SiO2 content: 30% by mass)) to obtain a mixed slurry of silica sol and aluminum nitrate. Subsequently, the mixed slurry was aged by holding at 50° C. for 24 hours. After cooling to room temperature, the mixed slurry was spray-dried with a spray dryer set to an outlet temperature of 130° C. to obtain a solid.

後処理

  1. additionwas gradually dropped into 20.0 kg of a stirred silica sol solution
  2. customheld at 15° C.

出典と根拠

ORDレコード
ord-5f8bc8bd92e44bda9fadb8d56b7ccf97
出典データセット
uspto-grants-2013_06
特許番号
US08461373B2

関連ノート

読み込み中…