Methylamine → HCID 20571388、化合物

HRID 126977

反応式

HRID 126977 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH:12]([CH3:14])[CH3:13])[C:9](O)=[O:10])=[CH:4][CH:3]=1.C(Cl)(=O)C(Cl)=O.[CH3:21][NH2:22]>>[CH3:21][NH:22][C:9](=[O:10])[CH:8]([C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=1)[CH:12]([CH3:14])[CH3:13]

参加物

4

反応物 3

HCID 6329MethylamineHCID 16197Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)-HCID 65578Oxalyl chloride

生成物 1

HCID 20571388HCID 20571388、化合物

実験手順

Following the methods of Example 1, 2-(4-chlorophenyl)-3-methylbutanoic acid is reacted with oxalyl chloride and aqueous methylamine to give N-methyl-2-(4-chlorophenyl)-3-methylbutyramide, which is then combined with 3-phenoxybenzyl bromide and AgBF4, yielding 3-phenoxybenzyl N-methyl-2-(4-chlorophenyl)-3-methylbutanimidate, MS m/e 407 (M+).

出典と根拠

ORDレコード
ord-f22e67409f3745d498d28c7d45897e05
出典データセット
uspto-grants-1981_03
特許番号
US04254264

関連ノート

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