Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride

HRID 1273

反応式

HRID 1273 の反応式
[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4](O)=[O:5].[Cl-:14]>>[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4]([Cl:14])=[O:5]

参加物

3

反応物 2

HCID 312ChlorideHCID 101303052-Methyl-3,4,6-trifluorobenzoic acid

生成物 1

HCID 150076072-Methyl-3,4,6-trifluorobenzoyl chloride

実験手順

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

後処理

  1. temperaturethe mixture is refluxed for 1 hour
  2. concentrationAfter concentrating

出典と根拠

ORDレコード
ord-141b4f862c4146f6950ca566cd749152
出典データセット
uspto-grants-1998_03
特許番号
US05723648

関連ノート

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