Chlorotrimethylsilane → HCID 12472499、化合物

HRID 1283094ノート

反応式

HRID 1283094 の反応式
[NH:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6].[CH3:7][Si:8]([CH3:11])([CH3:10])Cl.C(N(CC)CC)C>O1CCCC1>[CH3:7][Si:8]([CH3:11])([CH3:10])[N:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6]

参加物

5

反応物 3

HCID 6397ChlorotrimethylsilaneHCID 8471TriethylamineHCID 2723650Ethylenethiourea

生成物 1

HCID 12472499HCID 12472499、化合物

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried n a vacuum desiccator.

後処理

  1. filtrationThe warm suspension was freed of the precipitated triethylamine hydrochloride by filtration
  2. customthe filtrate was evaporated
  3. customdried n a vacuum desiccator

出典と根拠

ORDレコード
ord-ddd16d1308a0445783f6e24af410a5dd
出典データセット
uspto-grants-1976_08
特許番号
US03974140

反応ノート

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