Carbon Disulfide → 5-Hydroxypentyl isothiocyanate
反応式
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].[C:8](=S)=[S:9].C(N(CC)CC)C.C(Cl)(=O)OCC>C(Cl)(Cl)Cl>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]=[C:8]=[S:9]参加物
6
実験手順
The synthesis method of Example 45-(1) was applied. 5-Hydroxypentylamine (6.00 g), carbon disulfide (40 ml), triethylamine (8.3 ml), ethyl chlorocarbonate (5.4 ml), triethylamine (8.3 ml) and chloroform (20 ml) were used as reagents. After the reaction, a yellow liquid was quantitatively obtained.
後処理
- customThe synthesis method of Example 45-(1)
- customAfter the reaction
- customa yellow liquid was quantitatively obtained
出典と根拠
- ORDレコード
- ord-8df58fab982b4bcdb01a58c3cde4623e
- 出典データセット
- uspto-grants-1998_05
- 特許番号
- US05750545
反応ノート
読み込み中…