Acetonitrile → HCID 21889441、化合物

HRID 1352180ノート

反応式

HRID 1352180 の反応式
[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:15])[CH3:14])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([OH:22])(=[O:21])=[O:20])([CH3:3])[CH3:2].C(#N)C.[Ag:26]=O>CC(C)=O>[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:14])[CH3:15])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([O-:22])(=[O:21])=[O:20])([CH3:2])[CH3:3].[Ag+:26]

参加物

5

反応物 3

HCID 6342AcetonitrileHCID 92152Silver(II) oxideHCID 218894203-Nitro-2,4,6-tri(propan-2-yl)benzene-1-sulfonic acid

生成物 1

HCID 21889441HCID 21889441、化合物

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

Into a flask were charged 20 parts of 2,4,6-triisopropyl-3-nitrobenzenesulfonic acid, 80 parts of acetonitrile and 40 parts of acetone, and the mixture was stirred at room temperature for 16 hours. To this was added 7.46 parts of silver oxide, and the mixture was stirred at room temperature for 16 hours, and then filtered and concentrated to obtain 23.68 parts of silver 2,4,6-triisopropyl-3-nitrobenzenesulfonate.

後処理

  1. stirringthe mixture was stirred at room temperature for 16 hours
  2. filtrationfiltered
  3. concentrationconcentrated

出典と根拠

ORDレコード
ord-69941d1e013c4be3a0ce3a0526dd9244
出典データセット
uspto-grants-2007_05
特許番号
US07220532B2

反応ノート

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