Isopropylamine → 2-Amino-N-isopropylbenzamide
反応式
[C:1]12[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[NH:6]C(=O)[O:4][C:2]2=O.[CH:13]([NH2:16])([CH3:15])[CH3:14]>O>[NH2:6][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:1]=1[C:2]([NH:16][CH:13]([CH3:15])[CH3:14])=[O:4]参加物
4
実験手順
A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid
後処理
- customThe product precipitated from the reaction mixture
- filtrationthe reaction mixture was filtered
- washwashed with water
出典と根拠
- ORDレコード
- ord-7fc24b27a8664e549d66df96405fa8cf
- 出典データセット
- uspto-grants-2011_02
- 特許番号
- US07884098B2
反応ノート
読み込み中…