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Hydrochloric Acid → HCID 12540260、化合物

HRID 1413235
ノート
印刷プレビュー

反応式

HRID 1413235 の反応式
[H-].[Na+].[C:3]([O:11][CH2:12][CH3:13])(=[O:10])[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6].[CH:14]1([C:19]2([CH3:39])[CH2:27][C:26]3[C:21](=[C:22]([Cl:37])[C:23]([Cl:36])=[C:24](OS(C(F)(F)F)(=O)=O)[CH:25]=3)[C:20]2=[O:38])[CH2:18][CH2:17][CH2:16][CH2:15]1.Cl>CN(C)C=O.C(Cl)Cl>[CH:14]1([C:19]2([CH3:39])[CH2:27][C:26]3[C:21](=[C:22]([Cl:37])[C:23]([Cl:36])=[C:24]([CH:4]([C:5]([O:7][CH2:8][CH3:9])=[O:6])[C:3]([O:11][CH2:12][CH3:13])=[O:10])[CH:25]=3)[C:20]2=[O:38])[CH2:15][CH2:16][CH2:17][CH2:18]1
参加物実験手順後処理出典と根拠反応ノート

参加物

7

反応物 4

HCID 313Hydrochloric AcidHCID 7761Diethyl MalonateHCID 24758Sodium hydrideHCID 125402562-Cyclopentyl-6,7-dichloro-2-methyl-5-trifluoromethylsulfonyloxy-1-indanone

生成物 1

HCID 12540260HCID 12540260、化合物

試薬・触媒・溶媒 2

HCID 6228Dimethylformamide
溶媒
3 回
HCID 6344Dichloromethane溶媒

実験手順

To a stirred suspension of sodium hydride (2.88 g., 120 mmole) in dry dimethylformamide (20 ml), under dry nitrogen and cooled in an ice-bath is added dropwise, a solution of diethyl malonate (19.2 g., 120 mmole) in dimethylformamide (30 ml). The mixture is stirred for one hour in the ice-bath and another hour at room temperature, then is cooled in the ice-bath again and 2-cyclopentyl-6,7-dichloro-2-methyl-5-trifluoromethylsulfonyloxy-1-indanone (12.93 g., 30 mmole) in dimethylformamide (25 ml) is added dropwise over 1-1/2 hours. The mixture is stirred at room temperature overnight and then poured into a mixture of ice-water (750 ml), methylene chloride (200 ml) and 6 N hydrochloric acid (20 ml). The methylene chloride layer is separated and the aqueous layer extracted with methylene chloride (50 ml). The combined extract is washed with water (500 ml), dried (MgSO4) and evaporated under vacuum, finally at 70°/0.05 Torr, to give an oil (18.28 g.). This is purified by chromatography on Merck silica gel (1.04 Kg) using 1,1,1-trichloroethane as the solvent. The product is accompanied by some diethyl malonate which is removed at 125°/0.05 Torr to give a viscous oil, 10.25 g. (77%),

後処理

  1. temperatureunder dry nitrogen and cooled in an ice-bath
  2. additionis added dropwise
  3. customThe methylene chloride layer is separated
  4. extractionthe aqueous layer extracted with methylene chloride (50 ml)
  5. extractionThe combined extract
  6. washis washed with water (500 ml)
  7. dry with materialdried (MgSO4)
  8. customevaporated under vacuum, finally at 70°/0.05 Torr
  9. customto give an oil (18.28 g.)
  10. customThis is purified by chromatography on Merck silica gel (1.04 Kg)
  11. customis removed at 125°/0.05 Torr
  12. customto give a viscous oil, 10.25 g

出典と根拠

ORDレコード
ord-e43b951722024e148771017bc90dd902
出典データセット
uspto-grants-1981_02
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04249021

反応ノート

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