反応式
[Sb](F)(F)(F)(F)[F:2].FC(O[C:11]1[C:16]([CH3:17])=[CH:15][CH:14]=[CH:13][C:12]=1[CH3:18])=O>>[CH3:18][C:12]1[CH:13]=[CH:14][CH:15]=[C:16]([CH3:17])[C:11]=1[F:2]参加物
3
反応条件
- 温度
- 200 °C
実験手順
3.9 g of antimony pentafluoride were added to 100 g of 2,6-dimethylphenyl fluoroformate and the mixture was heated at 200° C. for 5 hours at normal pressure. The reaction mixture was then cooled and worked up as described in Example 1. 2,6-Dimethylfluorobenzene was obtained in a yield of 40%.
後処理
- temperatureThe reaction mixture was then cooled
出典と根拠
- ORDレコード
- ord-baa92f8612094a66b8c28eae6b5d3051
- 出典データセット
- uspto-grants-1994_04
- 特許番号
- US05306849
関連ノート
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