Ethanol → L-Carnitine Vinpocetine

HRID 1484008

反応式

HRID 1484008 の反応式
[OH:1][C@H:2]([CH2:8][C:9](=[O:11])[O-:10])[CH2:3][N+:4]([CH3:7])([CH3:6])[CH3:5].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.C(O)C.C(OC(C1C=CC(O)=CC=1)=O)C>OCC(CO)O>[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.[OH:1][C@H:2]([CH2:8][C:9](=[O:10])[O-:11])[CH2:3][N+:4]([CH3:7])([CH3:5])[CH3:6]

参加物

6

反応物 4

HCID 702EthanolHCID 8434EthylparabenHCID 10917(-)-CarnitineHCID 443955Vinpocetine

生成物 1

HCID 86298728L-Carnitine Vinpocetine

試薬・触媒・溶媒 1

HCID 753Glycerol溶媒

反応条件

温度
55 °C

実験手順

Process: Take L-carnitine and vinpocetine, add into ethanol and boil to completely dissolution, add ethylparaben and stir, and add defined amount of glycerin and stir uniformly, and then slowly add the solution into glycerinated gelatin substrate to preserve heat for later use. Add polysorbate and stir uniformly, and then slowly stir the solution and add into the said glycerinated gelatin substrate, stir well and preserve the heat at 55° C., and affuse into the membrane, and cool them down.

後処理

  1. dissolutionboil to completely dissolution
  2. additionadd
  3. stirringstir uniformly
  4. additionslowly add the solution
  5. temperatureto preserve heat for later use
  6. stirringslowly stir the solution
  7. additionadd into the
  8. stirringstir well
  9. temperaturecool them down

出典と根拠

ORDレコード
ord-6ec5712844be46cdb9bde30eea2ff6f8
出典データセット
uspto-grants-2016_08
特許番号
US09421181B2

関連ノート

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