N-Benzoylbenzylamine → N-benzyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
反応式
O=C(NCc1ccccc1)c1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1[nH]c2c(NC(=O)c3ccc(-c4ccccn4)nc3)cccc2c1C.[Ir].[Ir]>CC1(C)OB(c2ccccc2C(=O)NCc2ccccc2)OC1(C)C参加物
6
反応条件
- 温度
- 60 °C
実験手順
Isolated by chromatography using deactivated silica gel and ethyl acetate and petroleum ether (10:1 to 1:1) as the eluent.
出典と根拠
- ORDレコード
- ord-595736498a9142558380004d6497216a
- 出典データセット
- Borylation dataset from Roche
反応ノート
読み込み中…