Hydrochloric Acid → HCID 70274422、化合物

HRID 1586847ノート

反応式

HRID 1586847 の反応式
[CH3:1][CH2:2][CH:3]([S:6]([NH2:9])(=[O:8])=[O:7])[CH2:4][CH3:5].[OH-].[Na+].[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([N:19]=[C:20]=[O:21])=[CH:15][CH:14]=1.Cl>CC(C)=O.O>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][C:20]([NH:9][S:6]([CH:3]([CH2:4][CH3:5])[CH2:2][CH3:1])(=[O:8])=[O:7])=[O:21])=[CH:15][CH:14]=1

参加物

7

反応物 4

HCID 313Hydrochloric AcidHCID 76934-Chlorophenyl IsocyanateHCID 14798Sodium HydroxideHCID 22131302Pentane-3-sulfonamide

生成物 1

HCID 70274422HCID 70274422、化合物

試薬・触媒・溶媒 2

HCID 180Acetone溶媒3 回HCID 962Water溶媒

実験手順

The general method of procedure A was followed with 3-pentanesulfonamide (10 g), acetone (300 ml), 1N sodium hydroxide (56 ml), and 4-chlorophenyl isocyanate (9.6 g) dissolved in 70 ml of acetone. After two hours of stirring, 1N HCl (66 ml) was added followed by more water. The acetone was stripped off, and the resulting solid collected, to give, after drying at 65° C. under vacuum, 13.1 g of product.

後処理

  1. customthe resulting solid collected
  2. customto give
  3. dry with materialafter drying at 65° C. under vacuum, 13.1 g of product

出典と根拠

ORDレコード
ord-1a109a0adc0042daaa6e9855e6b21845
出典データセット
uspto-grants-1993_06
特許番号
US05216026

反応ノート

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