Hydroquinone → Dicumyl peroxide

HRID 1601477

反応式

HRID 1601477 の反応式
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].[C:9]1([CH:16]=[CH:15][C:13](O)=[CH:12][CH:11]=1)O.C[CH2:18][C:19]([O:23][O:24][C:25](OO)([CH2:27]C)[CH3:26])(OO)[CH3:20].CN(C)[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>ClCCl.C1(C)C=CC=CC=1>[C:19]([O:23][O:24][C:25]([C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)([CH3:27])[CH3:26])([C:9]1[CH:16]=[CH:15][CH:13]=[CH:12][CH:11]=1)([CH3:20])[CH3:18]

参加物

8

反応物 5

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

生成物 1

HCID 6641Dicumyl peroxide

試薬・触媒・溶媒 2

HCID 1140Toluene溶媒HCID 6344Dichloromethane溶媒

実験手順

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ehtyl ketone peroxide, dimethylaniline, dicumylperoxide were obtained from commercial sources and used as received.

出典と根拠

ORDレコード
ord-c184df2281e94453b3f0a43f9683210f
出典データセット
uspto-grants-1999_11
特許番号
US05977269

関連ノート

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