Azobisisobutyronitrile → Acrylic acid methyl acrylate

HRID 1610781

反応式

[C:1]([OH:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:10][CH3:11])(=[O:9])[CH:7]=[CH2:8].C(OC(C)COC)(=O)C.CC(N=NC(C#N)(C)C)(C#N)C>CC(CC(C)C)=O>[C:1]([OH:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:10][CH3:11])(=[O:9])[CH:7]=[CH2:8]

参加物

反応条件

温度: 67 °C

実験手順

9 g of acrylic acid, 1 g of methyl acrylate, 50 g of isobutyl methyl ketone, 50 g of propylene glycol methyl ether acetate and 3.0 g of AIBN were combined and heated to about 67° C. for 3 hours under an inert atmosphere (e.g., nitrogen gas). The precipitated polymer was washed with ethyl ether and vacuum dried to obtain pure poly(acrylic acid/methyl acrylate) resin (weight average molecular weight: 7200, yield: 54%).

後処理

washThe precipitated polymer was washed with ethyl ether and vacuum
customdried

出典と根拠

ORDレコード: ord-a2d1d2ff081c422e9147f0ad74d22d8a
出典データセット: uspto-grants-2006_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06984482B2

反応式

参加物

反応物 4

生成物 1

試薬・触媒・溶媒 1

反応条件

実験手順

後処理

出典と根拠

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