Tetrafluoroethylene → HCID 178447915、化合物

HRID 1653610

反応式

HRID 1653610 の反応式
[CH2:1]([C@H:4]1[CH2:9][CH2:8][C@H:7]([C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3].[H-].[Na+].[F:19][C:20]([F:24])=[C:21](F)[F:22]>C1C=CC=CC=1.O1CCCC1>[CH2:1]([C@H:4]1[CH2:5][CH2:6][C@H:7]([C:10]2[CH:15]=[CH:14][C:13]([O:16][C:21]([F:22])=[C:20]([F:24])[F:19])=[CH:12][CH:11]=2)[CH2:8][CH2:9]1)[CH2:2][CH3:3]

参加物

6

反応物 3

HCID 8301TetrafluoroethyleneHCID 24758Sodium hydrideHCID 178447901HCID 178447901、化合物

生成物 1

HCID 178447915HCID 178447915、化合物

試薬・触媒・溶媒 2

HCID 241Benzene溶媒HCID 8028Tetrahydrofuran溶媒

反応条件

温度
140 °C

実験手順

A solution of 10 g of p-(trans-4-n-propylcyclohexyl)phenol in a mixture of 40 ml of benzene and 10 ml of tetrahydrofuran is reacted with sodium hydride analogously to Example 1. After tetrafluoroethene has been condensed in, the mixture is heated at 140° C. for about 20 hours and treated as described in Example 1. p-(trans-4-n-propylcyclohexyl)trifluorovinyloxybenzene is obtained.

後処理

  1. customcondensed in, the mixture
  2. additiontreated

出典と根拠

ORDレコード
ord-ad8186fb5b77478cb16f6ce861a808d8
出典データセット
uspto-grants-1995_04
特許番号
US05403512

関連ノート

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