Ammonia → N,N-Dimethylaminopropyl acrylamide

HRID 1732222

反応式

HRID 1732222 の反応式
O[CH2:2][CH2:3][C:4]([NH2:6])=[O:5].[CH3:7][N:8]([CH3:13])[CH2:9][CH2:10][CH2:11]N.N.[OH-].[Na+]>>[CH3:7][N:8]([CH3:13])[CH2:9][CH2:10][CH2:11][NH:6][C:4](=[O:5])[CH:3]=[CH2:2]

参加物

5

反応物 4

HCID 222AmmoniaHCID 7993N,N-Dimethyl-1,3-propanediamineHCID 14798Sodium HydroxideHCID 41451403-Hydroxypropanamide

生成物 1

HCID 77452N,N-Dimethylaminopropyl acrylamide

実験手順

59.3 g of β-hydroxypropionic acid amide and 68 g of 3-dimethylaminopropylamine were heated for 5 hours in a temperature range of 125°-168° C. until the evolution of ammonia was complete. After adding 1 g of pulverised sodium hydroxide the reaction mixture was distilled.

後処理

  1. distillationwas distilled

出典と根拠

ORDレコード
ord-9fb2048b1977420aad17c78493b3ea51
出典データセット
uspto-grants-1980_12
特許番号
US04237067

関連ノート

読み込み中…