反応式
[CH2:1]([CH2:3][NH2:4])[OH:2].[ClH:5].[S:6]1(=[O:13])(=[O:12])[CH2:10][CH2:9][CH:8](N)[CH2:7]1>>[ClH:5].[OH:2][CH2:1][CH2:3][NH:4][CH:8]1[CH2:9][CH2:10][S:6](=[O:13])(=[O:12])[CH2:7]1参加物
3
実験手順
The procedure of Example 1 was repeated substituting 95 percent monoethanolamine (28.6 parts) for the ammonium hydroxide of Example 1. A sticky solid was filtered after treatment with hydrochloric acid, and upon drying in vacuo over P2O5 weighed 59.6 g. (78.5 percent of theory) m.p. 122°-124° C.
後処理
- filtrationA sticky solid was filtered after treatment with hydrochloric acid
- dry with materialupon drying in vacuo over P2O5
出典と根拠
- ORDレコード
- ord-86cb4db8a7b940b4a64ef7d396ff5961
- 出典データセット
- uspto-grants-1983_02
- 特許番号
- US04374040
関連ノート
読み込み中…