Hydrochloric Acid → HCID 85866484、化合物

HRID 1763188

反応式

HRID 1763188 の反応式
[CH3:1][N:2]1[CH2:7]N(C)CN(C)C1.[C:10]([S:18]CN)([CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:12])[CH3:11].[ClH:21]>C(#N)C>[ClH:21].[CH3:1][NH:2][CH2:7][S:18][C:10]([CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:12])[CH3:11]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 79521,3,5-Trimethyl-1,3,5-triazacyclohexaneHCID 86735983HCID 86735983、化合物

生成物 1

HCID 85866484HCID 85866484、化合物

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

300 ml. of acetonitrile, 12.9 g. (0.1 mole) of 1,3,5-trimethylhexahydro-s-triazine; 43.8 g. (0.3 mole) of tert.-octylthiomethylamine and 12 g. of hydrogen chloride gas are reacted together in the manner of Example I. A yield of 43.7 g. (64.6% of theory) of the title compound is obtained.

出典と根拠

ORDレコード
ord-dba2278fae3647809136087c4a36efe9
出典データセット
uspto-grants-1978_09
特許番号
US04111682

関連ノート

読み込み中…