Glycine → Glycine, N,N-bis(2-cyanoethyl)- (8CI)(9CI)

反応式

[C:1](#[N:4])[CH:2]=[CH2:3].[Na].[NH2:6][CH2:7][C:8]([OH:10])=[O:9]>>[C:1]([CH2:2][CH2:3][N:6]([CH2:3][CH2:2][C:1]#[N:4])[CH2:7][C:8]([OH:10])=[O:9])#[N:4]

参加物

反応物 3

HCID 750Glycine

HCID 7855Acrylonitrile

HCID 5360545Sodium2 回

生成物 1

HCID 80523Glycine, N,N-bis(2-cyanoethyl)- (8CI)(9CI)

実験手順

Bis-cyanoethyl glycine was prepared in conventional manner by reacting two mols acrylonitrile with one mol sodium salt of glycine in essentially the same manner used in preparing the catalyst of Example 2, except that the sodium salt was neutralized at the end of the reaction.

出典と根拠

ORDレコード: ord-f8dcaa48958e420a92f7366218c3aa9c
出典データセット: uspto-grants-1978_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04115634

反応ノート

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