Formaldehyde → 3-(Hydroxymethyl)-4-methylpent-4-en-2-one
反応式
[O:1]=[C:2]([CH:4]=[C:5]([CH3:7])[CH3:6])[CH3:3].[CH2:8]=[O:9]>>[CH3:6][C:5]([CH:4]([CH2:8][OH:9])[C:2](=[O:1])[CH3:3])=[CH2:7]参加物
3
実験手順
The reaction is carried out at temperatures between 20° and 130° C. The reaction time is, for example, 3 hours at 30° C and a few minutes at 100° C. Advantageously, the mesityl oxide and catalyst are initially introduced and formaldehyde is metered in. The 2-methyl-3-hydroxymethyl-pent-1-en-4-one can be isolated from the reaction mixture by, for example, distillation, advantageously after neutralising the basic catalyst.
後処理
- customis carried out at temperatures between 20° and 130° C
- customis, for example, 3 hours at 30° C and a few minutes at 100° C
出典と根拠
- ORDレコード
- ord-3faeea22ff9d4aed965cd4e97dc45972
- 出典データセット
- uspto-grants-1978_01
- 特許番号
- US04069257
反応ノート
読み込み中…