Succinic anhydride → HCID 86585086、化合物

反応式

[CH2:1]([OH:7])/[CH:2]=[CH:3]/[CH:4]=[CH:5]/[CH3:6].[C:8]1(=[O:14])[O:13][C:11](=[O:12])[CH2:10][CH2:9]1>>[C:8]([OH:13])(=[O:14])[CH2:9][CH2:10][C:11]([OH:7])=[O:12].[CH2:1]([OH:7])/[CH:2]=[CH:3]/[CH:4]=[CH:5]/[CH3:6]

参加物

反応物 2

HCID 7922Succinic anhydride

HCID 641256trans,trans-2,4-Hexadien-1-ol

生成物 1

HCID 86585086HCID 86585086、化合物

実験手順

Trans,trans-hexa-2,4-dien-1-ol and succinic anhydride are reacted in the presence of N,N-dimethylaminopyridine to provide trans,trans-hexa-2,4-dien-1-ol monosuccinate. An aqueous solution of an excess of the monosuccinate is activated with 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide and coupled with human serum albumin, to provide a poly(diene) derivative 11.

出典と根拠

ORDレコード: ord-2803042c6de24c4b8cf9111f06875d1c
出典データセット: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06673905B2

反応ノート

読み込み中…