Hydrochloric Acid → HCID 70274422、化合物

HRID 1857580ノート

反応式

HRID 1857580 の反応式
[CH3:1][CH2:2][CH:3]([S:6]([NH2:9])(=[O:8])=[O:7])[CH2:4][CH3:5].[OH-].[Na+].[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([N:19]=[C:20]=[O:21])=[CH:15][CH:14]=1.Cl>CC(C)=O.O>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][C:20]([NH:9][S:6]([CH:3]([CH2:4][CH3:5])[CH2:2][CH3:1])(=[O:8])=[O:7])=[O:21])=[CH:15][CH:14]=1

参加物

7

反応物 4

HCID 313Hydrochloric AcidHCID 76934-Chlorophenyl IsocyanateHCID 14798Sodium HydroxideHCID 22131302Pentane-3-sulfonamide

生成物 1

HCID 70274422HCID 70274422、化合物

試薬・触媒・溶媒 2

HCID 180Acetone溶媒3 回HCID 962Water溶媒

実験手順

The general method of procedure A was followed with 3-pentanesulfonamide (10 g), acetone (300 ml), 1N sodium hydroxide (56 ml), and 4-chlorophenyl isocyanate (9.6 g) dissolved in 70 ml of acetone. After two hours of stirring, 1N HCl (66 ml) was added followed by more water. The acetone was stripped off, and the resulting solid collected, to give, after drying at 65° C. under vacuum, 13.1 g of product.

後処理

  1. customthe resulting solid collected
  2. customto give
  3. dry with materialafter drying at 65° C. under vacuum, 13.1 g of product

出典と根拠

ORDレコード
ord-6a094da47c8342ec8ab7da94d80b7250
出典データセット
uspto-grants-2000_11
特許番号
US06147115

反応ノート

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