反応式
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=O.[C:8]([O:12][CH2:13][CH2:14][N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])(=[O:11])[CH:9]=[CH2:10].C1N2CCN(CC2)C1.[O:28]1CCOCC1>>[OH:4][CH:1]([CH3:2])[O:5][C:6]([CH2:7][C:9](=[CH2:10])[C:8]([O:12][CH2:13][CH2:14][N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])=[O:11])=[O:28]参加物
5
実験手順
51 g (0.5 mole) of ethyl glyoxylate, 85.5 g (0.5 mole) of N,N-diethylaminoethyl acrylate and 5 g (62.5 millimoles) of DABCO in 100 ml of absolute dioxane are reacted by a method similar to that described in Example 6. 74 g (54% of theory) of diethylaminoethyl 2-(1-hydroxycarbethoxymethyl)-acrylate are obtained.
出典と根拠
- ORDレコード
- ord-72f6b8d625a8495f9d1d729303c6e6ec
- 出典データセット
- uspto-grants-1987_03
- 特許番号
- US04652669
関連ノート
読み込み中…