Dimethylcarbamoyl Chloride → HCID 54349798、化合物

HRID 1957358ノート

反応式

HRID 1957358 の反応式
[CH3:1][N:2]([CH3:6])[C:3](Cl)=[O:4].[N:7]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]=[N:14][N:15]2[CH:19]=[N:18][NH:17][C:16]2=[O:20])[CH:8]=1>N1C=CC=CC=1>[CH3:1][N:2]([CH3:6])[C:3]([N:17]1[C:16](=[O:20])[N:15]([N:14]=[CH:13][C:9]2[CH:8]=[N:7][CH:12]=[CH:11][CH:10]=2)[CH:19]=[N:18]1)=[O:4]

参加物

4

反応物 2

HCID 6598Dimethylcarbamoyl ChlorideHCID 54560653HCID 54560653、化合物

生成物 1

HCID 54349798HCID 54349798、化合物

試薬・触媒・溶媒 1

HCID 1049Pyridine溶媒

実験手順

3.2 g of dimethylcarbamoyl chloride are added to a suspension of 3.8 g of 4-(pyridin-3-ylmethyleneamino)-1,2,4-triazol-3-one in 50 ml of pyridine. The resulting solution is stirred for 14 hours at 20° and then concentrated by evaporation. Water is added to the residue. The crystals that have precipitated are filtered off with suction and dried under a high vacuum. 3.6 g of crystals of the title compound having a melting point of 181°-182° are obtained.

後処理

  1. concentrationconcentrated by evaporation
  2. additionWater is added to the residue
  3. customThe crystals that have precipitated
  4. filtrationare filtered off with suction
  5. customdried under a high vacuum
  6. customare obtained

出典と根拠

ORDレコード
ord-6daa293bfc534d1abeca111e8331732b
出典データセット
uspto-grants-1998_07
特許番号
US05783704

反応ノート

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