Methyl iodide → HCID 178480658、化合物

HRID 1959998

反応式

HRID 1959998 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.[CH3:13][I:14]>C1COCC1>[I-:14].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH3:13])[CH:9]=2)=[CH:6][CH:7]=1

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 1428591-(4-Chlorophenyl)-1H-imidazole

生成物 1

HCID 178480658HCID 178480658、化合物

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.

後処理

  1. customThe precipitate formed
  2. filtrationis subsequently filtered off
  3. washwashed with ethanol and with petroleum ether
  4. customsubsequently dried under reduced pressure

出典と根拠

ORDレコード
ord-5ba2519728b1474aaa39a8a35afc3e46
出典データセット
uspto-grants-2013_04
特許番号
US08410280B2

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