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Sodium Carbonate → Dichromium tricarbonate

HRID 2039358
ノート
印刷プレビュー

反応式

HRID 2039358 の反応式
[C:1](=[O:4])([O-:3])[O-:2].[Na+].[Na+].[Cl-].[Cr+3:8].[Cl-].[Cl-]>>[C:1](=[O:2])([O-:4])[O-:3].[Cr+3:8].[C:1](=[O:2])([O-:4])[O-:3].[C:1](=[O:2])([O-:4])[O-:3].[Cr+3:8]
参加物実験手順後処理出典と根拠反応ノート

参加物

3

反応物 2

HCID 10340Sodium Carbonate3 回HCID 6452300Chromium(3+) trichloride4 回

生成物 1

HCID 165489Dichromium tricarbonate

実験手順

500 g of a 10% aqueous solution of sodium carbonate and 86.4 g of a 35% aqueous solution of chromium chloride (manufactured by Nippon Chemical Industrial Co., Ltd.) were each placed in a container and prepared. Next, the aqueous solution of sodium carbonate and the aqueous solution of chromium chloride were adjusted to a reaction temperature of 20° C. Unlike Example 1, the aqueous solution of sodium carbonate was added to the aqueous solution of chromium chloride at a speed of 10 g/min, while the aqueous solution of chromium chloride was stirred. The produced precipitate was filtered and washed with water to obtain a chromium (III) carbonate cake. This chromium (III) carbonate cake was dried in a vacuum at 40° C. for 48 hours to obtain a blue-green chromium (III) carbonate powder. Measurement as in Example 1 was performed for this chromium (III) carbonate. The results are shown in the following Table 3. However, the solubility was measured only immediately after the production.

後処理

  1. customprepared
  2. customwere adjusted to a reaction temperature of 20° C
  3. filtrationThe produced precipitate was filtered
  4. washwashed with water

出典と根拠

ORDレコード
ord-c7b119892cd1463aa7397ecf78324617
出典データセット
uspto-grants-2013_11
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08580221B2

反応ノート

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