Sodium Carbonate Decahydrate → Pentabromodiphenyl ethers

HRID 2058053

反応式

HRID 2058053 の反応式
[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1.P(OC1C=CC=CC=1)(OC1C=CC=CC=1)(OCC(CC)CCCC)=O.O.O.O.O.O.O.O.O.O.O.C(=O)([O-])[O-].[Na+].[Na+]>O>[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1

参加物

4

反応物 2

HCID 151402Sodium Carbonate DecahydrateHCID 131711832HCID 131711832、化合物

生成物 1

HCID 36159Pentabromodiphenyl ethers

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Using the procedure of Examples II and IV, the pentabromodiphenyl ether-2-ethylhexyl diphenyl phosphate blend was heated to 130° C., and sodium carbonate decahydrate (2.7% W/W on the blend) was added and subjected to agitation in the closed system for one-half hour. Thereafter, the system was opened in order to permit water to escape. The molten mixture was filtered to obtain the purified blend. Relevant properties of the blend are given in Table III.

後処理

  1. waitsubjected to agitation in the closed system for one-half hour
  2. filtrationThe molten mixture was filtered
  3. customto obtain the purified blend

出典と根拠

ORDレコード
ord-e3755f6f64ff4cec9d58fbca0c3ac339
出典データセット
uspto-grants-1980_07
特許番号
US04214103

関連ノート

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