S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride → Dibenzylamine
反応式
Cl.[CH2:2]([N:9](CCCCSC(=N)N)[CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>[OH-].[Na+]>[CH2:10]([NH:9][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1参加物
3
実験手順
S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride (prepared according to Example 15) was hydrolysed in aqueous ethanolic sodium hydroxide. The solvents were evaporated and the residue taken up in water and extracted 3 times with methylene dichloride. The extracts were dried (MgSO4), filtered and evaporated to give N-(3-mercaptopropy])dibenzylamine.
後処理
- customThe solvents were evaporated
- extractionextracted 3 times with methylene dichloride
- dry with materialThe extracts were dried (MgSO4)
- filtrationfiltered
- customevaporated
出典と根拠
- ORDレコード
- ord-dfd2f0be67984e6aabe343adb657573f
- 出典データセット
- uspto-grants-1995_06
- 特許番号
- US05422355
反応ノート
読み込み中…