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Acetone → (Phenylmethyl) [5-[2-[4-(4-morpholinyl)phenyl]ethoxy] pentyl]carbamate

HRID 2166164
ノート
印刷プレビュー

反応式

HRID 2166164 の反応式
Cl[C:2]([O:4][CH2:5][CH3:6])=[O:3].C[C:8](C)([CH2:12][CH2:13][CH2:14][CH2:15][O:16][CH2:17][CH2:18][C:19]1[CH:24]=[CH:23][C:22]([N:25]2[CH2:30][CH2:29][O:28][CH2:27][CH2:26]2)=[CH:21][CH:20]=1)C(O)=O.C(N([CH2:37][CH3:38])CC)C.[N-:39]=[N+]=[N-].[Na+].[CH3:43][C:44]([CH3:46])=O>O>[N:25]1([C:22]2[CH:21]=[CH:20][C:19]([CH2:18][CH2:17][O:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:8][NH:39][C:2](=[O:3])[O:4][CH2:5][C:6]3[CH:38]=[CH:37][CH:46]=[CH:44][CH:43]=3)=[CH:24][CH:23]=2)[CH2:26][CH2:27][O:28][CH2:29][CH2:30]1
参加物実験手順後処理出典と根拠反応ノート

参加物

7

反応物 5

HCID 180Acetone2 回HCID 8471TriethylamineHCID 10928Ethyl chloroformateHCID 33557Sodium AzideHCID 200628192,2-Dimethyl-6-[2-[4-(4-morpholinyl)phenyl]ethoxy]hexanoic acid

生成物 1

HCID 53892071(Phenylmethyl) [5-[2-[4-(4-morpholinyl)phenyl]ethoxy] pentyl]carbamate

試薬・触媒・溶媒

1
HCID 962Water溶媒3 回

実験手順

Ethyl chloroformate (3.29 g) in acetone (10 ml) was added dropwise to a solution of the product of stage (iii) (10.0 g) and triethylamine (3.0 g, 30 mmol) in acetone (100 ml) and water (10 ml) at 0°. The mixture was stirred at 0° for 40 min and sodium azide (2.0 g) in water (25 ml) was added dropwise. The resulting suspension was stirred at room temperature for 45 min, diluted with water (200 ml) and extracted with T (2×200 ml). The dried (Na2SO4) extract was heated at 75°-80° for 2.5 h and evaporated. The residue was treated with benzyl alcohol (20 ml), heated at 75°-80° for 60 h and benzyl alcohol was removed by distillation (~1 mmHg). The resulting oil was purified on a column of silica (Merck 9385) eluted with ER-CX (1:2) to give the title compound, as a yellow oil (4.74 g). T.l.c. ER-CX (1:2) Rf 0.13.

後処理

  1. stirringThe resulting suspension was stirred at room temperature for 45 min
  2. extractionextracted with T (2×200 ml)
  3. dry with materialThe dried (Na2SO4)
  4. extractionextract
  5. temperaturewas heated at 75°-80° for 2.5 h
  6. customevaporated
  7. additionThe residue was treated with benzyl alcohol (20 ml)
  8. temperatureheated at 75°-80° for 60 h
  9. custombenzyl alcohol was removed by distillation (~1 mmHg)
  10. customThe resulting oil was purified on a column of silica (Merck 9385)
  11. washeluted with ER-CX (1:2)

出典と根拠

ORDレコード
ord-89c3f088cd774184ba4f1c7e1fff7f2c
出典データセット
uspto-grants-1990_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04943591

反応ノート

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