Propylene Oxide → Propylene oxide butylene oxide

HRID 2184627

反応式

HRID 2184627 の反応式
C(O)C(O)[CH2:3][O:4][CH2:5][CH:6]([OH:9])[CH2:7]O.[OH-].[K+].C1OC1C>C1OCCC1>[CH2:7]1[O:9][CH:6]1[CH3:5].[CH2:3]1[O:4][CH2:5][CH2:6][CH2:7]1

参加物

5

反応物 3

HCID 6378Propylene OxideHCID 14797Potassium HydroxideHCID 42953Diglycerin

生成物 1

HCID 22138293Propylene oxide butylene oxide

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

166 g of a starting substance, diglycerin, 32 g of a catalyst, potassium hydroxide, 9,290 g of propylene oxide, and 1,460 g of butylene oxide were put into a 15-L autoclave, and reacted at 110° C. for 16 hours, and then neutralized, desalted and purified to obtain 9,900 g of a tetra-functional propylene oxide-butylene oxide copolymer. This polymer had a molecular weight of 10,900 (as calculated from its hydroxyl value).

後処理

  1. customreacted at 110° C. for 16 hours
  2. custompurified

出典と根拠

ORDレコード
ord-22fc703fc6ff4d6c990dbe51abac4b40
出典データセット
uspto-grants-2002_06
特許番号
US06399254B1

関連ノート

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