Hydrogen Bromide → HCID 178515992、化合物

HRID 2216339

反応式

HRID 2216339 の反応式
[CH2:1]([C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([O:14]C)[N:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br>O>[CH2:1]([C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([OH:14])[N:9]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

参加物

4

反応物 2

HCID 260Hydrogen BromideHCID 219422742-Benzyl-6-methoxypyridine

生成物 1

HCID 178515992HCID 178515992、化合物収率 70.9%

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
100 °C

実験手順

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.

後処理

  1. temperaturewas heated
  2. temperatureto cool
  3. filtrationthe resulting crystals were filtered
  4. washwashed with water
  5. customdried under reduced pressure

出典と根拠

ORDレコード
ord-8432c46a7bbf42feb057a7de3b73cea2
出典データセット
uspto-grants-2006_09
特許番号
US07112593B2

関連ノート

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