反応式
Cl[C:2]1[CH:9]=[CH:8][C:7]([N+:10]([O-])=O)=[CH:6][C:3]=1[C:4]#[N:5].[CH3:13][N:14]1[CH2:19][CH2:18][NH:17][CH2:16][CH2:15]1>>[NH2:10][C:7]1[CH:8]=[CH:9][C:2]([N:17]2[CH2:18][CH2:19][N:14]([CH3:13])[CH2:15][CH2:16]2)=[C:3]([CH:6]=1)[C:4]#[N:5]参加物
3
実験手順
By the reaction and treatment in the same manner as in Starting Material Synthetic Example 4 using 2-chloro-5-nitrobenzonitrile (15 g) and methylpiperazine (9.8 g), the title compound (11.1 g) was obtained. melting point: 45-46° C.
後処理
- customBy the reaction and treatment in the same manner as
出典と根拠
- ORDレコード
- ord-58fcb8b3c4f747289de79d546576b89c
- 出典データセット
- uspto-grants-2006_09
- 特許番号
- US07112594B2
関連ノート
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