Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid

HRID 2227019

反応式

HRID 2227019 の反応式
FC1C=C[C:5]([CH:8]2[O:13]C(=O)CC(=O)[O:9]2)=CC=1.[CH:16](=O)[C:17]1[CH:26]=[CH:25][C:22]([O:23][CH3:24])=[C:19]([O:20][CH3:21])[CH:18]=1.C(O)=O>C(N(CC)CC)C>[CH3:21][O:20][C:19]1[CH:18]=[C:17]([CH2:16][CH2:5][C:8]([OH:13])=[O:9])[CH:26]=[CH:25][C:22]=1[O:23][CH3:24]

参加物

5

実験手順

5.26 g (0.025 mol) of 2-(4-fluorophenyl)-1,3-dioxane-4,6-dione (m.p.: 166°-167° C.) and 4.15 g (0.025 mol) of veratraldehyde were added to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction was carried out according to Example 1.

後処理

  1. customprepared

出典と根拠

ORDレコード
ord-93ad8b5c70aa4baeb0248dd498d8ee07
出典データセット
uspto-grants-1994_09
特許番号
US05350872

関連ノート

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