Water → Adipic Acid

HRID 223583

反応式

HRID 223583 の反応式
C(OC(C1C=CC=CC=1)[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)C.C1C=CC(C(N=C=O)N=[C:27]=[O:28])=CC=1.[C:32]([O:37]CCO)(=[O:36])[C:33]([CH3:35])=C.[OH2:41]>C(O)C>[C:5]([OH:12])(=[O:28])[CH2:6][CH2:11][CH2:35][CH2:33][C:32]([OH:37])=[O:36].[C:32]([OH:37])(=[O:36])[C:11]1[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=1)[C:5]([OH:12])=[O:41].[CH2:27]([C:6]([CH2:5][OH:12])([CH2:7][OH:36])[CH2:11][CH3:10])[OH:28]

参加物

8

反応物 4

HCID 962WaterHCID 133602-Hydroxyethyl MethacrylateHCID 101778Benzoin ethyl etherHCID 12905475Diisocyanatotoluene

生成物 3

HCID 196Adipic AcidHCID 1017Phthalic AcidHCID 6510Trimethylolpropane

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

1.2 A 12% strength solution of a mixture of 2 parts of benzoin ethyl ether, 6 parts of the reaction product of 1 mole of toluylene diisocyanate and 2 moles of β-hydroxyethyl methacrylate and 92 parts of the polyvinyl alcohol/methacrylic anhydride reaction product, prepared as described in 1.1, in a mixture of equal parts of water and ethanol is prepared. The solution is applied to a steel sheet which has been coated with a polyurethane adhesive according to German Laid-Open Application DOS No. 1,597,515 (prepared from a commercial hydroxy-containing polyester, obtained from 2.5 moles of adipic acid, 0.5 mole of phthalic acid and 4 moles of 1,1,1-trimethylolpropane, by reaction with a triisocyanate prepared by reacting 3 moles of toluylene diisocyanate with 1 mole of 1,1,1-trimethylolpropane), the amount of solution applied to the sheet being such that, after curing for 7 minutes in a cabinet dryer at 150° C., a 10 μm thick intermediate layer (c) results.

後処理

  1. customprepared
  2. customis prepared

出典と根拠

ORDレコード
ord-3a9014de7a3646218300cd7665d36f73
出典データセット
uspto-grants-1982_10
特許番号
US04355093

関連ノート

読み込み中…