反応式
O.[N:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][C:9]#[N:10].[CH:11](=O)[CH:12]([CH3:14])[CH3:13].N1CCCCC1>C1C=CC=CC=1.C(O)(=O)C>[CH3:11][CH:12]([CH3:14])[CH:13]=[C:8]([C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][N:2]=1)[C:9]#[N:10]参加物
7
実験手順
In a flask equipped with a water separator are placed 7 g of 2-pyridyl acetonitrile, 12.8 g of isobutyraldehyde, 0.9 ml of acetic acid, 0.18 ml of piperidine and 250 ml of dry benzene. The mixture is heated under reflux for 3 hours. After cooling, the reaction mixture is washed with water, the organic phase is dried over sodium sulfate then the solvent is evaporated to dryness.
後処理
- temperatureThe mixture is heated
- temperatureunder reflux for 3 hours
- temperatureAfter cooling
- washthe reaction mixture is washed with water
- dry with materialthe organic phase is dried over sodium sulfate
- customthe solvent is evaporated to dryness
出典と根拠
- ORDレコード
- ord-8c24038a3fed4ea884fea50cdda5a581
- 出典データセット
- uspto-grants-1982_10
- 特許番号
- US04356177
関連ノート
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